{"database":"biostudies-literature","file_versions":[],"scores":null,"additional":{"omics_type":["Unknown"],"submitter":["Aalling-Frederiksen O"],"funding":["Carlsbergfondet","Danmarks Grundforskningsfond","European Research Council","Deutsche Forschungsgemeinschaft","Villum Fonden"],"pubmed_abstract":["We here investigate how the synthesis method affects the crystallite size and atomic structure of cobalt iron oxide nanoparticles. By using a simple solvothermal method, we first synthesized cobalt ferrite nanoparticles of <i>ca.</i> 2 and 7 nm, characterized by Transmission Electron Microscopy (TEM), Small Angle X-ray scattering (SAXS), X-ray and neutron total scattering. The smallest particle size corresponds to only a few spinel unit cells. Nevertheless, Pair Distribution Function (PDF) analysis of X-ray and neutron total scattering data shows that the atomic structure, even in the smallest nanoparticles, is well described by the spinel structure, although with significant disorder and a contraction of the unit cell parameter. These effects can be explained by the surface oxidation of t"],"journal":["Nanoscale advances"],"full_dataset_link":["https://www.ebi.ac.uk/biostudies/studies/S-EPMC11443383"],"repository":["biostudies-literature"],"pubmed_title":["Effect of solvothermal synthesis parameters on the crystallite size and atomic structure of cobalt iron oxide nanoparticles."],"pmcid":["PMC11443383"],"funding_grant_id":["408076438","804066","VKR00015416","DNRF 149","818941","CF21-0278"],"pubmed_authors":["Anker AS","Frandsen BA","Klemeyer L","Pittkowski RK","Jensen KMO","Aalling-Frederiksen O","Koziej D","Quinson J"],"additional_accession":[]},"is_claimable":false,"name":"Effect of solvothermal synthesis parameters on the crystallite size and atomic structure of cobalt iron oxide nanoparticles.","description":"We here investigate how the synthesis method affects the crystallite size and atomic structure of cobalt iron oxide nanoparticles. By using a simple solvothermal method, we first synthesized cobalt ferrite nanoparticles of <i>ca.</i> 2 and 7 nm, characterized by Transmission Electron Microscopy (TEM), Small Angle X-ray scattering (SAXS), X-ray and neutron total scattering. The smallest particle size corresponds to only a few spinel unit cells. Nevertheless, Pair Distribution Function (PDF) analysis of X-ray and neutron total scattering data shows that the atomic structure, even in the smallest nanoparticles, is well described by the spinel structure, although with significant disorder and a contraction of the unit cell parameter. These effects can be explained by the surface oxidation of t","dates":{"release":"2024-01-01T00:00:00Z","publication":"2024 Sep","modification":"2026-07-17T01:05:44.511Z","creation":"2026-07-12T03:12:25.809Z"},"accession":"S-EPMC11443383","cross_references":{"pubmed":["39364296"],"doi":["10.1039/d4na00590b"]}}