biostudies-literatureZoubir OMinisterio de Ciencia, Innovación y Universidadeslaboratory at Faculty of Science, Mohammed V University in Rabat1329https://www.ebi.ac.uk/biostudies/studies/S-EPMC11943971biostudies-literatureUnknown18(6)The sodium super ionic conductor (NASICON) structured LiTi<sub>2</sub>(PO<sub>4</sub>)<sub>3</sub> (LTP) has been developed as electrode material for Li-ion batteries (LIBs) with promising electrochemical performance, owing to its outstanding structural stability and rapid lithium-ion diffusion. Nevertheless, challenges still exist, especially the rapid capacity fading caused by the low electronic conductivity of LTP-NASICON material. Recently, the hydrothermal method has emerged as an important technique for the production of diverse nano-electrode materials due to its low preparation temperature, high phase purity, and well-controlled morphology and crystallinity. Herein, we report, for the first time at low-moderate temperatures, an advanced hydrothermal synthesis of LTP-coated reduced Materials (Basel, Switzerland)In-Situ One-Step Hydrothermal Synthesis of LiTi&lt;sub&gt;2&lt;/sub&gt;(PO&lt;sub&gt;4&lt;/sub&gt;)&lt;sub&gt;3&lt;/sub&gt;@rGO Anode for High Performance Lithium-Ion Batteries.PMC11943971MCIN/AEI/10.13039/501100011033 Projects PID2020-113931RB-I00 & PID2023-147080OB-I00MANAPSEZoubir OTesio AYCaballero AEdfouf ZOubla MLallaoui AfalseIn-Situ One-Step Hydrothermal Synthesis of LiTi&lt;sub&gt;2&lt;/sub&gt;(PO&lt;sub&gt;4&lt;/sub&gt;)&lt;sub&gt;3&lt;/sub&gt;@rGO Anode for High Performance Lithium-Ion Batteries.The sodium super ionic conductor (NASICON) structured LiTi<sub>2</sub>(PO<sub>4</sub>)<sub>3</sub> (LTP) has been developed as electrode material for Li-ion batteries (LIBs) with promising electrochemical performance, owing to its outstanding structural stability and rapid lithium-ion diffusion. Nevertheless, challenges still exist, especially the rapid capacity fading caused by the low electronic conductivity of LTP-NASICON material. Recently, the hydrothermal method has emerged as an important technique for the production of diverse nano-electrode materials due to its low preparation temperature, high phase purity, and well-controlled morphology and crystallinity. Herein, we report, for the first time at low-moderate temperatures, an advanced hydrothermal synthesis of LTP-coated reduced 2025-01-01T00:00:00Z2025 Mar2025-07-09T03:04:38.422Z2025-07-09T03:04:38.422ZS-EPMC119439714014161210.3390/ma18061329