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Novel Synthesis of 3D Mesoporous FePO₄ from Electroflocculation of Iron Filings as a Precursor of High-Performance LiFePO₄/C Cathode for Lithium-Ion Batteries.

ABSTRACT: This study presents an economic and environmentally friendly method for the synthesis of microspherical FePO₄·2H₂O precursors with secondary nanostructures by the electroflocculation of low-cost iron fillers in a hot solution. The morphology and crystalline shape of the precursors were adjusted by gradient co-precipitation of pH conditions. The effect of precursor structure and morphology on the electrochemical performance of the synthesized LiFePO₄/C was investigated. Electrochemical analysis showed that the assembly of FePO₄·2H₂O submicron spherical particles from primary nanoparticles and nanorods resulted in LiFePO₄/C exhibiting excellent multiplicity and cycling performance with first discharge capacities at 0.2C, 1C, 5

SUBMITTER: Peng J

PROVIDER: S-EPMC10099130 | biostudies-literature | 2023 Apr

REPOSITORIES: biostudies-literature

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Novel Synthesis of 3D Mesoporous FePO₄ from Electroflocculation of Iron Filings as a Precursor of High-Performance LiFePO₄/C Cathode for Lithium-Ion Batteries.

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Novel Synthesis of 3D Mesoporous FePO4 from Electroflocculation of Iron Filings as a Precursor of High-Performance LiFePO4/C Cathode for Lithium-Ion Batteries.

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Novel Synthesis of 3D Mesoporous FePO₄ from Electroflocculation of Iron Filings as a Precursor of High-Performance LiFePO₄/C Cathode for Lithium-Ion Batteries.