Effect of Manganese Distribution on Sensor Properties of SnO₂/MnO_x Nanocomposites.

ABSTRACT: Nanocomposites SnO₂/MnO_x with various manganese content (up to [Mn]/[Sn] = 10 mol. %) and different manganese distribution were prepared by wet chemical technique and characterized by X-ray diffraction, scanning electron microscopy (SEM) with energy dispersive X-ray (EDX) analysis and mapping, IR and Raman spectroscopy, total reflection X-ray fluorescence, mass-spectrometry with inductive-coupled plasma (ICP-MS), X-ray photoelectron spectroscopy (XPS), electron paramagnetic resonance (EPR) spectroscopy. A different distribution of manganese between the volume and the surface of the SnO₂ crystallites was revealed depending on the total Mn concentration. Furthermore, the identification of surface MnO₂ segregation was performed via Raman spectroscop

SUBMITTER: Eshmakov R 

PROVIDER: S-EPMC10179853 | biostudies-literature | 2023 Apr

REPOSITORIES: biostudies-literature