Structure and Photocatalytic Properties of Ni-, Co-, Cu-, and Fe-Doped TiO₂ Aerogels.

ABSTRACT: TiO₂ aerogels doped with Ni, Co, Cu, and Fe were prepared, and their structure and photocatalytic activity during the decomposition of a model pollutant, acid orange (AO7), were studied. After calcination at 500 °C and 900 °C, the structure and composition of the doped aerogels were evaluated and analyzed. XRD analysis revealed the presence of anatase/brookite and rutile phases in the aerogels along with other oxide phases from the dopants. SEM and TEM microscopy showed the nanostructure of the aerogels, and BET analysis showed their mesoporosity and high specific surface area of 130 to 160 m²·g^-1. SEM-EDS, STEM-EDS, XPS, EPR methods and FTIR analysis evaluated the presence of dopants and their chemical state. The concentration of doped metals in aerogels v

SUBMITTER: Lizeth Katherine TN 

PROVIDER: S-EPMC10217561 | biostudies-literature | 2023 Apr

REPOSITORIES: biostudies-literature