Systematic Study of the Multiple Variables Involved in V₂AlC Acid-Based Etching Processes, a Key Step in MXene Synthesis.

ABSTRACT: The realization of the broad range of application of MXenes relies on the successful and reproducible synthesis of quality materials of tailored properties. To date, most MXenes have been produced making use of acid-based etching methods, yet an in-depth understanding of etching processes is lacking. Herein, we have engaged in a comprehensive study of the multiple variables involved in the synthesis of V₂CT_x with focus on the properties of etched materials. Two main sets of experiments were considered, each using a different V₂AlC precursor and a range of synthesis variables including reaction time and temperature, mixing rate, and type of acid. Correlations of synthesis conditions-materials properties were investigated using a broad range of charact

SUBMITTER: Mendoza-Sanchez B 

PROVIDER: S-EPMC10273183 | biostudies-literature | 2023 Jun

REPOSITORIES: biostudies-literature