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Chitosan and Its Carboxymethyl-Based Membranes Produced by Crosslinking with Magnesium Phytate.


ABSTRACT: Membranes produced by crosslinking chitosan with magnesium phytate were prepared using highly deacetylated chitosan and its N-carboxymethyl, O-carboxymethyl and N,O-carboxymethyl derivatives. The conditions of the membrane production were described. IR, Raman, electron absorption and emission spectra were measured and analyzed for all the substrates. It was found that O-carboxymethyl chitosan derivative is the most effectively crosslinked by magnesium phytate, and the films formed on this substrate exhibit good mechanical parameters of strength, resistance and stability. Strong O-H···O hydrogen bonds proved to be responsible for an effective crosslinking process. Newly discovered membrane types produced from chitosan and magnesium phytate were characterized as morphologically homogenous and uniform by scanning electron microscopy (SEM) and IR measurements. Due to their good covering properties, they do not have pores or channels and are proposed as packaging materials.

SUBMITTER: Zajac A 

PROVIDER: S-EPMC10459599 | biostudies-literature | 2023 Aug

REPOSITORIES: biostudies-literature

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Chitosan and Its Carboxymethyl-Based Membranes Produced by Crosslinking with Magnesium Phytate.

Zając Adam A   Sąsiadek Wojciech W   Dymińska Lucyna L   Ropuszyńska-Robak Paulina P   Hanuza Jerzy J   Ptak Maciej M   Smółka Szymon S   Lisiecki Radosław R   Skrzypczak Katarzyna K  

Molecules (Basel, Switzerland) 20230810 16


Membranes produced by crosslinking chitosan with magnesium phytate were prepared using highly deacetylated chitosan and its <i>N</i>-carboxymethyl, <i>O</i>-carboxymethyl and <i>N</i>,<i>O</i>-carboxymethyl derivatives. The conditions of the membrane production were described. IR, Raman, electron absorption and emission spectra were measured and analyzed for all the substrates. It was found that <i>O</i>-carboxymethyl chitosan derivative is the most effectively crosslinked by magnesium phytate,  ...[more]

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