ABSTRACT: In this work, we investigated in detail the upconversion properties of several types of nanoparticles, including NaYF4:5%Yb3+/30%Mn2+, NaYF4:40%Mn2+/x%Yb3+ (x% = 1, 5, 10, 20, 30, and 40), NaYF4:2%Er3+/x%Mn2+ (x% = 20, 30, 40, 50, 60, and 70), NaYF4:40%Mn2+/x%Er3+ (x% = 1, 2, 5, and 10), and NaYF4:40%Mn2+/1%Yb3+/x%Er3+ (x% = 0, 2, 5, and 10). We studied their upconversion emission under 980 nm excitation in both pulsed and continuous wave modes at different synthesis temperatures. The nanoparticles were characterized using transmission electron microscopy (TEM), X-ray diffraction (XRD), and photoluminescence (PL) spe