Hydrothermal synthesis of hierarchical microstructure tungsten oxide/carbon nanocomposite for supercapacitor application.
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ABSTRACT: A hierarchical nanocomposite of carbon microspheres decorated with tungsten oxide (WO3) nanocrystals resulted from the hydrothermal treatment of a precursor solution containing glucose and tungstic acid. The dehydration of glucose molecules formed oligosaccharides, which consequently carbonized, turning into carbon microspheres. The carbon microspheres then acted as a spherical nucleus onto which WO3 nanocrystals grew via heterogeneous nucleation. The reaction product showed a phase junction of orthorhombic and monoclinic WO3, which transitioned to mix-phase of tetragonal and monoclinic WO3 after a subsequent heat treatment at 600 °C in an inert condition. The electrochemical tests showed that incorporating WO3 onto the carbon (WO3/C) resulted in a three-fold increase in the specific capac
SUBMITTER: Alonzo SMM
PROVIDER: S-EPMC10709354 | biostudies-literature | 2023 Dec
REPOSITORIES: biostudies-literature
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