Nanomaterials Synthesis Discovery via Parallel Electrochemical Deposition.

ABSTRACT: Electrodeposition of nanoparticles is investigated with a multichannel potentiostat in electrochemical and chemical arrays. De novo deposition and shape control of palladium nanoparticles are explored in arrays with a two-stage strategy. Initial conditions for electrodeposition of materials are discovered in a first stage and then used in a second stage to logically expand chemical and electrochemical parameters. Shape control is analyzed primarily with scanning electron microscopy. Using this approach, optimized conditions for the electrodeposition of cubic palladium nanoparticles were identified from a set of previously untested electrodeposition conditions. The parameters discovered through the array format were then successfully extrapolated to a traditional bulk three-electrode

SUBMITTER: Personick ML 

PROVIDER: S-EPMC10976633 | biostudies-literature | 2024 Mar

REPOSITORIES: biostudies-literature