A complete 3D-printed tool kit for Solid-State NMR sample and rotor handling.

ABSTRACT: Solid state NMR (SSNMR) is a highly versatile and broadly applicable method for studying the structure and dynamics of biomolecules and materials. For scientists entering the field of SSNMR, the many quotidian activities required in the workflow to prepare samples for data collection can present a significant barrier to adoption. These steps include transfer of samples into rotors, marking the reflective surfaces for high sensitivity tachometer signal detection, inserting rotors into the magic-angle spinning (MAS) stator, achieving stable spinning, and removing and storing rotors to ensure reproducibility of data collection conditions. Even experienced spectroscopists experience occasional problems with these operations, and the cumulative probability of a delay to successful data collecti

SUBMITTER: Olson MA 

PROVIDER: S-EPMC11423700 | biostudies-literature | 2024 Sep

REPOSITORIES: biostudies-literature