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Electrospun Iridium-Based Nanofiber Catalysts for Oxygen Evolution Reaction: Influence of Calcination on Activity-Stability Relation.


ABSTRACT: The enhanced utilization of noble metal catalysts through highly porous nanostructures is crucial to advancing the commercialization prospects of proton exchange membrane water electrolysis (PEMWE). In this study, hierarchically structured IrOx-based nanofiber catalyst materials for acidic water electrolysis are synthesized by electrospinning, a process known for its scalability and ease of operation. A calcination study at various temperatures from 400 to 800 °C is employed to find the best candidates for both electrocatalytic activity and stability. Morphology, structure, phase, and chemical composition are investigated using a scale-bridging approach by SEM, TEM, XRD, and XPS to shed light on the structure-function relationship of the thermally prepared nanofibers. Act

SUBMITTER: Kovacs MM 

PROVIDER: S-EPMC11450683 | biostudies-literature | 2024 Oct

REPOSITORIES: biostudies-literature