The Synergic Effect of h-MoO₃, α-MoO₃, and β-MoO₃ Phase Mixture as a Solid Catalyst to Obtain Methyl Oleate.

ABSTRACT: Extensive research in the last few decades has conclusively demonstrated the significant influence of experimental conditions, surfactants, and synthesis methods on semiconductors' properties in technological applications. Therefore, in this study, the synthesis of molybdenum oxide (MoO₃) was reported by the addition of 2.5 (MoO₃_2.5), 5 (MoO₃_5), 7.5 (MoO₃_7.5), and 10 mL (MoO₃_10) of nitric acid, obtaining the respective concentrations of 0.6, 1.10, 1.6, and 0.6 mol L^-1. In this study, all samples were synthesized by the hydrothermal method at 160 °C for 6 h. The materials obtained were structurally characterized by X-ray diffraction (XRD) and structural Rietveld refinement, Raman spectroscopy, and infrared spectroscopy (F

SUBMITTER: Medeiros Leao GS 

PROVIDER: S-EPMC11551912 | biostudies-literature | 2024 Nov

REPOSITORIES: biostudies-literature