Controlled bottom-up synthesis and characterization of crystalline and amorphous lead(II) coordination polymers: Sonochemical methods, structure-property relationship, and photocatalytic applications.
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ABSTRACT: The 3D coordination polymers of lead (II) [Pb4(O)(L)3(H2O)]n, where H2L = C6H4(CO2H)2 (benzene-1,3-dicarboxylic acid), were synthesized in crystalline (1(a, b)) and amorphous (2(a, b)) phases. Hydrothermal and branch tube methods were used to self-assemble lead (II) from the bottom up to create the crystalline phases. Single-crystal X-ray diffraction (SC-XRD) was used to investigate two crystallized metal-organic frameworks (MOFs) with the same space group and chemical formula (P21/c). Through controlled green sonochemical methods, an ultrasonic bath and a probe homogenizer were used to prepare nano [Pb4(O)(L)3(H2O)]n in the amorphous phase. An extensive study has been c
SUBMITTER: Sichani SE
PROVIDER: S-EPMC11869037 | biostudies-literature | 2025 Mar
REPOSITORIES: biostudies-literature
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