Electrochemical Liquid Phase TEM in Aqueous Electrolytes for Energy Applications: the Role of Liquid Flow Configuration.

ABSTRACT: Electrochemical liquid phase transmission electron microscopy (EC-LPTEM) is an invaluable tool for investigating the structural and morphological properties of functional materials in electrochemical systems for energy transition. Despite its potential, standardized experimental protocols and a consensus on data interpretation are lacking, due to a variety of commercial and customized electrical and microfluidic configurations. Given the small size of a typical electrochemical cell used in these experiments, frequent electrolyte renewal is crucial to minimize local chemical alterations from reactions and radiolysis. This study explores the effects of modifying the flow configuration within the liquid cell under experimental conditions relevant for energy applications in aqueous-based elect

SUBMITTER: Bejtka K 

PROVIDER: S-EPMC11926486 | biostudies-literature | 2025 Mar

REPOSITORIES: biostudies-literature