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1,4-Bis(piperidin-1-ylcarbon-yl)benzene.

ABSTRACT: The title compound, C(18)H(20)N(2)O(2), has been synthesized by the reaction of terephthaloyl chloride and 1,2,3,6-tetra-hydro-pyridine. This compound crystallizes as discrete mol-ecular species disposed about a crystallographic centre of symmetry, such that half the mol-ecule constitutes the asymmetric unit. The structure shows an envelope conformation for the dehydro-piperidine ring with the amide carbonyl twisted out of the benzene ring plane by 57.3 (2)°.

SUBMITTER: Armbrust L

PROVIDER: S-EPMC2914991 | biostudies-literature | 2007 Dec

REPOSITORIES: biostudies-literature

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1,4-Bis(piperidin-1-ylcarbon-yl)benzene.

Armbrust Lee L Bilyk Alex A Brown Christopher L CL Healy Peter C PC

Acta crystallographica. Section E, Structure reports online 20071206 Pt 1

The title compound, C(18)H(20)N(2)O(2), has been synthesized by the reaction of terephthaloyl chloride and 1,2,3,6-tetra-hydro-pyridine. This compound crystallizes as discrete mol-ecular species disposed about a crystallographic centre of symmetry, such that half the mol-ecule constitutes the asymmetric unit. The structure shows an envelope conformation for the dehydro-piperidine ring with the amide carbonyl twisted out of the benzene ring plane by 57.3 (2)°. ...[more]

PMID: 21200873

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