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1,2-Bis(1,3-benzothia-zol-2-yl)benzene.

ABSTRACT: The title compound, C(20)H(12)N(2)S(2), was prepared by the reaction of o-phthalic acid and 2-amino-thio-phenol under microwave irradation. The phenyl ring, A, and the benzothia-zolyl rings, B and C, are planar; the dihedral angles are A/B = 19.9 (11), A/C = 87.8 (3) and B/C = 84.4 (4)°. Weak inter-molecular C-H⋯N hydrogen bonds link the mol-ecule, forming zigzag chains parallel to the c axis.

SUBMITTER: Wang GW 

PROVIDER: S-EPMC2968071 | biostudies-literature | 2008 Dec

REPOSITORIES: biostudies-literature

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1,2-Bis(1,3-benzothia-zol-2-yl)benzene.

Wang Guo-Wei GW   Wu Lin-Ping LP   Zhuang Ling-Hua LH   Wang Jin-Tang JT  

Acta crystallographica. Section E, Structure reports online 20081220 Pt 1

The title compound, C(20)H(12)N(2)S(2), was prepared by the reaction of o-phthalic acid and 2-amino-thio-phenol under microwave irradation. The phenyl ring, A, and the benzothia-zolyl rings, B and C, are planar; the dihedral angles are A/B = 19.9 (11), A/C = 87.8 (3) and B/C = 84.4 (4)°. Weak inter-molecular C-H⋯N hydrogen bonds link the mol-ecule, forming zigzag chains parallel to the c axis. ...[more]

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