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N,N'-Bis(3-chloro-phen-yl)malonamide.

ABSTRACT: The asymmetric unit of the title compound, C(15)H(12)Cl(2)N(2)O(2), contains two independent mol-ecules. In both independent mol-ecules, the N-H bond in one of the amide fragments is anti to the meta-chloro group of the adjacent benzene ring and that in the other amide group is syn to the other meta-chloro group. Furthermore, in both mol-ecules, each amide group is almost coplanar with the adjacent phenyl ring, making dihedral angles of 10.5 (2) and 8.7 (2)° in one molecule and 9.0 (2) and 9.6 (2)° in the other. The planes of the amide groups are inclined at dihedral angles of 83.4 (1) and 87.4 (1)° in the two mol-ecules. In the crystal, mol-ecules are linked into a chain by inter-molecular N-H⋯O hydrogen bonds.

SUBMITTER: Rodrigues VZ 

PROVIDER: S-EPMC3200632 | biostudies-literature | 2011 Sep

REPOSITORIES: biostudies-literature

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N,N'-Bis(3-chloro-phen-yl)malonamide.

Rodrigues Vinola Z VZ   Foro Sabine S   Gowda B Thimme BT  

Acta crystallographica. Section E, Structure reports online 20110811 Pt 9

The asymmetric unit of the title compound, C(15)H(12)Cl(2)N(2)O(2), contains two independent mol-ecules. In both independent mol-ecules, the N-H bond in one of the amide fragments is anti to the meta-chloro group of the adjacent benzene ring and that in the other amide group is syn to the other meta-chloro group. Furthermore, in both mol-ecules, each amide group is almost coplanar with the adjacent phenyl ring, making dihedral angles of 10.5 (2) and 8.7 (2)° in one molecule and 9.0 (2) and 9.6 (  ...[more]

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