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1-[(2-Hy-droxy-phen-yl)(pyrrolidin-1-yl)-meth-yl]naphthalen-2-ol N,N-dimethyl-formamide monosolvate.

ABSTRACT: The title compound, C(21)H(21)NO(2)·C(3)H(7)NO, was synthesized by solvent-free one-pot three-component reaction of naphthalen-2-ol, 2-hy-droxy-benzaldehyde and pyrrolidine. The dihedral angle between the naphthalene ring system and the benzene ring is 77.74 (6)°. The pyrrolidine ring assumes an envelope conformation. An intra-molecular O-H⋯N and an inter-molecular O-H⋯O hydrogen bond are observed.

SUBMITTER: Wang WX

PROVIDER: S-EPMC3297932 | biostudies-literature | 2012 Mar

REPOSITORIES: biostudies-literature

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1-[(2-Hy-droxy-phen-yl)(pyrrolidin-1-yl)-meth-yl]naphthalen-2-ol N,N-dimethyl-formamide monosolvate.

Wang Wen-Xiang WX

Acta crystallographica. Section E, Structure reports online 20120229 Pt 3

The title compound, C(21)H(21)NO(2)·C(3)H(7)NO, was synthesized by solvent-free one-pot three-component reaction of naphthalen-2-ol, 2-hy-droxy-benzaldehyde and pyrrolidine. The dihedral angle between the naphthalene ring system and the benzene ring is 77.74 (6)°. The pyrrolidine ring assumes an envelope conformation. An intra-molecular O-H⋯N and an inter-molecular O-H⋯O hydrogen bond are observed. ...[more]

PMID: 22412735

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