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Nanoporous composites prepared by a combination of SBA-15 with Mg-Al mixed oxides. Water vapor sorption properties.


ABSTRACT: This work presents two easy ways for preparing nanostructured mesoporous composites by interconnecting and combining SBA-15 with mixed oxides derived from a calcined Mg-Al hydrotalcite. Two different Mg-Al hydrotalcite addition procedures were implemented, either after or during the SBA-15 synthesis (in situ method). The first procedure, i.e., the post-synthesis method, produces a composite material with Mg-Al mixed oxides homogeneously dispersed on the SBA-15 nanoporous surface. The resulting composites present textural properties similar to the SBA-15. On the other hand, with the second procedure (in situ method), Mg and Al mixed oxides occur on the porous composite, which displays a cauliflower morphology. This is an important microporosity contribution and micro and mesoporous surfaces

SUBMITTER: Perez-Verdejo A 

PROVIDER: S-EPMC4143113 | biostudies-literature | 2014

REPOSITORIES: biostudies-literature