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Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon-yl)amino]-butanoic acid.

ABSTRACT: The title compound, C15H17NO4S, was synthesized from l-valine and naphthalene-1-sulfonyl chloride. The hydrogen-bonded carb-oxy-lic acid groups form a catemer C(4) motif extending along [100]. The catemer structure is reinforced by a rather long N-H⋯O hydrogen bond, between the sulfamide N-H group and a carb-oxy-lic acid O atom [H⋯O = 2.52 (2) Å], and a C-H⋯O hydrogen bond.

SUBMITTER: Danish M 

PROVIDER: S-EPMC4420138 | biostudies-literature | 2015 May

REPOSITORIES: biostudies-literature

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Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon-yl)amino]-butanoic acid.

Danish Muhammad M   Tahir Muhammad Nawaz MN   Jabeen Nabila N   Raza Muhammad Asam MA  

Acta crystallographica. Section E, Crystallographic communications 20150415 Pt 5

The title compound, C15H17NO4S, was synthesized from l-valine and naphthalene-1-sulfonyl chloride. The hydrogen-bonded carb-oxy-lic acid groups form a catemer C(4) motif extending along [100]. The catemer structure is reinforced by a rather long N-H⋯O hydrogen bond, between the sulfamide N-H group and a carb-oxy-lic acid O atom [H⋯O = 2.52 (2) Å], and a C-H⋯O hydrogen bond. ...[more]

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