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Sealed rotors for in situ high temperature high pressure MAS NMR.

ABSTRACT: Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.

SUBMITTER: Hu JZ 

PROVIDER: S-EPMC4544657 | biostudies-literature | 2015 Sep

REPOSITORIES: biostudies-literature

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Sealed rotors for in situ high temperature high pressure MAS NMR.

Hu Jian Zhi JZ   Hu Mary Y MY   Zhao Zhenchao Z   Xu Suochang S   Vjunov Aleksei A   Shi Hui H   Camaioni Donald M DM   Peden Charles H F CH   Lercher Johannes A JA  

Chemical communications (Cambridge, England) 20150901 70

Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue. ...[more]

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