Absolute Configuration Determination of Retroflexanone Using the Advanced Mosher Method and Application of HPLC-NMR.

ABSTRACT: The absolute configuration of retroflexanone (1) and a closely related phlorogluinol (2) was established using the advanced Mosher method and by application of HPLC-NMR. HPLC-NMR permitted a small scale Mosher method analysis to be carried out on these unstable phloroglucinols.

SUBMITTER: Singleton C 

PROVIDER: S-EPMC6025468 | biostudies-literature | 2018 Jun

REPOSITORIES: biostudies-literature