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Eco-friendly synthesis of VO2 with stripped pentavalent vanadium solution extracted from vanadium-bearing shale by hydrothermal process in high conversion rate.


ABSTRACT: VO2(B) has shown excellent cathode performance in lithium batteries and become a hot research topic in recent years. A stripped vanadium solution extracted from vanadium-bearing shale containing a high concentration of vanadium and certain amounts of impurities was used as a vanadium source to synthesize VO2(B) by hydrothermal process. The VO2 conversion rate can reach as high as 99.47% in a reaction time of 8 h, and this is the highest result reported. The crystalline structure and morphology of the synthesized products were characterized by X-ray diffraction (XRD), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Scanning electron microscopy (SEM) and Transmission electron microscopy (TEM). Furthermore, the electrochemical properties of VO2(B) in lithium-ion batteries were inv

SUBMITTER: Kang Q 

PROVIDER: S-EPMC6408403 | biostudies-literature | 2019 Feb

REPOSITORIES: biostudies-literature