Two-Step Exfoliation of WS₂ for NO₂, H₂ and Humidity Sensing Applications.

ABSTRACT: WS₂ exfoliated by a combined ball milling and sonication technique to produce few-layer WS₂ is characterized and assembled as chemo-resistive NO₂, H₂ and humidity sensors. Microstructural analyses reveal flakes with average dimensions of 110 nm, "aspect ratio" of lateral dimension to the thickness of 27. Due to spontaneous oxidation of exfoliated WS₂ to amorphous WO₃, films have been pre-annealed at 180 °C to stabilize WO₃ content at ≈58%, as determined by X-ray Photoelectron Spectroscopy (XPS), Raman and grazing incidence X-ray Diffraction (XRD) techniques. Microstructural analysis repeated after one-year conditioning highlighted that amorphous WO₃ concentration is stable, attesting the validity of the

SUBMITTER: Paolucci V 

PROVIDER: S-EPMC6835748 | biostudies-literature | 2019 Sep

REPOSITORIES: biostudies-literature