Crystal structure and Hirshfeld surface analysis of 4-{[(anthracen-9-yl)meth-yl]amino}-benzoic acid di-methyl-formamide monosolvate.

ABSTRACT: The title compound, C₂₂H₁₇NO₂·C₃H₇NO, was synthesized by condensation of an aromatic aldehyde with a secondary amine and subsequent reduction. It was crystallized from a di-methyl-formamide solution as a monosolvate, C₂₂H₁₇NO₂·C₃H₇NO. The aromatic mol-ecule is non-planar with a dihedral angle between the mean planes of the aniline moiety and the methyl anthracene moiety of 81.36 (8)°. The torsion angle of the C_ar-yl-CH₂-NH-C_ar-yl backbone is 175.9 (2)°. The crystal structure exhibits a three-dimensional supra-molecular network, resulting from hydrogen-bonding inter-actions between the carb-oxy-lic OH group and the solvent O atom as well as between t

SUBMITTER: Ahmed A 

PROVIDER: S-EPMC7199275 | biostudies-literature | 2020 May

REPOSITORIES: biostudies-literature