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Synthesis of TiO2/WO3 Composite Nanofibers by a Water-Based Electrospinning Process and Their Application in Photocatalysis.


ABSTRACT: TiO2/WO3 nanofibers were prepared in a one-step process by electrospinning. Titanium(IV) bis(ammonium lactato)dihydroxide (TiBALDH) and ammonium metatungstate (AMT) were used as water-soluble Ti and W precursors, respectively. Polyvinylpyrrolidone (PVP) and varying ratios of TiBALDH and AMT were dissolved in a mixture of H2O, EtOH and CH3COOH. The as-spun fibers were then heated in air at 1 °C min-1 until 600 °C to form TiO2/WO3 composite nanofibers. Fiber characterization was done using TG/DTA, SEM-EDX, FTIR, XRD, and Raman. The annealed composite nanofibers had a diameter range of 130-1940 nm, and the results showed a growth in the fiber diameter with an increasing amount of WO3. The photocatalytic property of the fibers was also checked for methyl orange bleaching in visible and UV ligh

SUBMITTER: Odhiambo VO 

PROVIDER: S-EPMC7279266 | biostudies-literature | 2020 May

REPOSITORIES: biostudies-literature