Readily Constructed Glass Piston Pump for Gas Recirculation.

ABSTRACT: The recirculation of gases in a sealed reactor system is a broadly useful method in catalytic and electrocatalytic studies. It is especially relevant when a reactant gas reacts slowly with respect to residence time in a catalytic reaction zone and when mass transport control through the reaction zone is necessary. This need is well illustrated in the field of electrocatalytic N₂ reduction, where the need for recirculation of ¹⁵N₂ has recently become more apparent. Herein, we describe the design, fabrication, use, and specifications of a lubricant-free, readily constructed recirculating pump fabricated entirely from glass and inert polymer (poly(ether ether ketone) (PEEK), poly(tetrafluoroethylene) (PTFE)) components. Using these glass and polymer components

SUBMITTER: Nielander AC 

PROVIDER: S-EPMC7364576 | biostudies-literature | 2020 Jul

REPOSITORIES: biostudies-literature