Low-Temperature Synthesis of Monolithic Titanium Carbide/Carbon Composite Aerogel.

ABSTRACT: Resorcinol-formaldehyde/titanium dioxide composite (RF/TiO2) gel was prepared simultaneously by acid catalysis and then dried to aerogel with supercritical fluid CO2. The carbon/titanium dioxide aerogel was obtained by carbonization and then converted to nanoporous titanium carbide/carbon composite aerogel via 800 °C magnesiothermic catalysis. Meanwhile, the evolution of the samples in different stages was characterized by X-ray diffraction (XRD), an energy-dispersive X-ray (EDX) spectrometer, a scanning electron microscope (SEM), a transmission electron microscope (TEM) and specific surface area analysis (BET). The results showed that the final product was nanoporous TiC/C composite aerogel with a low apparent density of 339.5 mg/cm3 and a high specific surface area of 459.5 m2/g. Compari

SUBMITTER: Niu T 

PROVIDER: S-EPMC7767110 | biostudies-literature | 2020 Dec

REPOSITORIES: biostudies-literature