Effect of the Size and Shape of Ho, Tm:KLu(WO4)2 Nanoparticles on Their Self-Assessed Photothermal Properties.
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ABSTRACT: The incorporation of oleic acid and oleylamine, acting as organic surfactant coatings for a novel solvothermal synthesis procedure, resulted in the formation of monoclinic KLu(WO4)2 nanocrystals. The formation of this crystalline phase was confirmed structurally from X-ray powder diffraction patterns and Raman vibrational modes, and thermally by differential thermal analysis. The transmission electron microscopy images confirm the nanodimensional size (~12 nm and ~16 nm for microwave-assisted and conventional autoclave solvothermal synthesis) of the particles and no agglomeration, contrary to the traditional modified sol-gel Pechini methodology. Upon doping with holmium (III) and thulium (III) lanthanide ions, these nanocrystals can generate simultaneously photolumine
SUBMITTER: Nexha A
PROVIDER: S-EPMC7918361 | biostudies-literature | 2021 Feb
REPOSITORIES: biostudies-literature
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