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Crystal structure and Hirshfeld surface analysis of poly[[bis-[μ₄-N,N'-(1,3,5-oxadiazinane-3,5-di-yl)bis(carbamoyl-methano-ato)]nickel(II)tetra-potassium] 4.8-hydrate].

ABSTRACT: The title compound, {[K₄Ni₂(C₇H₆N₄O₇)₂]·4.8H₂O} _n , was obtained as a result of a template reaction between oxalohydrazide-hydroxamic acid, formaldehyde and nickel(II) nitrate followed by partial hydrolysis of the formed inter-mediate. The two independent [Ni(C₇H₆N₄O₇)]^2- complex anions exhibit pseudo-C _S symmetry and consist of an almost planar metal-containing fragment and a 1,3,5-oxadiazinane ring with a chair conformation disposed nearly perpendicularly with respect to the former. The central Ni^II atom has a square-planar N₂O₂ coordination arrangement formed by two amide N and

SUBMITTER: Plutenko MO

PROVIDER: S-EPMC8061116 | biostudies-literature | 2021 Mar

REPOSITORIES: biostudies-literature

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Crystal structure and Hirshfeld surface analysis of poly[[bis-[μ₄-N,N'-(1,3,5-oxadiazinane-3,5-di-yl)bis(carbamoyl-methano-ato)]nickel(II)tetra-potassium] 4.8-hydrate].

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Crystal structure and Hirshfeld surface analysis of poly[[bis-[μ4-N,N'-(1,3,5-oxadiazinane-3,5-di-yl)bis(carbamoyl-methano-ato)]nickel(II)tetra-potassium] 4.8-hydrate].

OmicsDI is part of the ELIXIR infrastructure

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Crystal structure and Hirshfeld surface analysis of poly[[bis-[μ₄-N,N'-(1,3,5-oxadiazinane-3,5-di-yl)bis(carbamoyl-methano-ato)]nickel(II)tetra-potassium] 4.8-hydrate].