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LiNa3(SO4)2·6H2O: a lithium double salt causing trouble in the industrial conversion of Li2SO4 into LiOH.

ABSTRACT: Lithium tris-odium bis-(sulfate) hexa-hydrate, LiNa3(SO4)2·6H2O was crystallized from aqueous solution at 298 K and the structure solved at different temperatures between 90 and 293 K. The structure is isomorphic with the corresponding molybdate and selenate double salt hydrate. It belongs to the non-centrosymmetric trigonal space group R3c (161). The temperature dependence of the lattice parameters has been determined. Further characterization by powder XRD and thermal analysis is reported.

SUBMITTER: Schmidt H 

PROVIDER: S-EPMC8423005 | biostudies-literature | 2021 Sep

REPOSITORIES: biostudies-literature

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LiNa<sub>3</sub>(SO<sub>4</sub>)<sub>2</sub>·6H<sub>2</sub>O: a lithium double salt causing trouble in the industrial conversion of Li<sub>2</sub>SO<sub>4</sub> into LiOH.

Schmidt Horst H   Paschke Iris I   Voigt Wolfgang W  

Acta crystallographica. Section E, Crystallographic communications 20210810 Pt 9

Lithium tris-odium bis-(sulfate) hexa-hydrate, LiNa<sub>3</sub>(SO<sub>4</sub>)<sub>2</sub>·6H<sub>2</sub>O was crystallized from aqueous solution at 298 K and the structure solved at different temperatures between 90 and 293 K. The structure is isomorphic with the corresponding molybdate and selenate double salt hydrate. It belongs to the non-centrosymmetric trigonal space group <i>R</i>3<i>c</i> (161). The temperature dependence of the lattice parameters has been determined. Further characteri  ...[more]

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