Strategies towards simpler configuration and higher peak capacity with comprehensive multidimensional gas chromatography.

ABSTRACT: Experimental and data analysis approaches in multidimensional gas chromatography (MDGC) comprising comprehensive multiple heart-cut (H/C) and comprehensive two dimensional GC (GC × GC) were developed with an example application illustrated for analysis of a technical glycol precursor sample. The GC × GC system employed a long ¹D (30 m) and a short ²D (5 m) column with a flow modulator and a Deans switch (DS) as a splitter; meanwhile. The H/C system was applied solely as a DS located between long ¹D (30 m) and ²D (60 m) columns without use of cryogenic trapping devices. The effects of injection time and ²D column flow in GC × GC and the impacts of H/C window and number of injections (total analysis time) in H/C analysis were investigate

SUBMITTER: Janta P 

PROVIDER: S-EPMC8695086 | biostudies-literature | 2021 Feb

REPOSITORIES: biostudies-literature