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Mechanical power driven SPME-SERS ultra-fast detection of illegal additives in aquaculture water.

ABSTRACT: A dual-function (extraction and detection) porous silver fiber with high enhancement effect was constructed based on a convenient electrochemical etching method. The prepared silver fiber not only had high enrichment capacity and good Surface Enhanced Raman Spectroscopy (SERS) performance but also had good laser stability and uniformity. A strategy combining mechanical power and integration of solid phase extraction (SPME) and SERS detection was used. Driven by mechanical power, the analyte malachite green (MG) was enriched on the prepared silver fiber after 40 seconds, which can realize an ultra-fast and sensitive detection with a detection limit of 8.48 × 10^-9 M. At the same time, this fiber can be regenerated after being treated with NaBH₄. The silver fiber can be used for the detection of MG and CV after being immersed in NaBH₄ solution for a few minutes. After 5 cycles of processing, the measurement signals of the silver fiber can reach 70% of the initial signals. The mechanical power driven SPME-SERS (MPD-SPME-SERS) integrated detection method can be used to analyse aquaculture water within 1 minute with a good linear relationship.

SUBMITTER: Lv H

PROVIDER: S-EPMC8697362 | biostudies-literature | 2021 Mar

REPOSITORIES: biostudies-literature

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Mechanical power driven SPME-SERS ultra-fast detection of illegal additives in aquaculture water.

Lv Handi H Guan Qi Q Wang Ying Y Zhang Xiaoli X

RSC advances 20210301 21

A dual-function (extraction and detection) porous silver fiber with high enhancement effect was constructed based on a convenient electrochemical etching method. The prepared silver fiber not only had high enrichment capacity and good Surface Enhanced Raman Spectroscopy (SERS) performance but also had good laser stability and uniformity. A strategy combining mechanical power and integration of solid phase extraction (SPME) and SERS detection was used. Driven by mechanical power, the analyte mala ...[more]

PMID: 35423820

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Project description:BackgroundMechanical power (MP) refers to the energy transmitted over time to the respiratory system and serves as a unifying determinant of ventilator-induced lung injury. MP normalization is required to account for developmental changes in children. We sought to examine the relationship between mechanical energy (MEBW), MP normalized to body weight (MPBW), and MP normalized to respiratory compliance (MPCRS) concerning the severity and outcomes of pediatric acute respiratory distress syndrome (pARDS).MethodIn this retrospective study, children aged 1 month to 18 years diagnosed with pARDS who underwent pressure-control ventilation for at least 24 h between January 2017 and September 2020 were enrolled. We calculated MP using Becher's equation. Multivariable logistic regression analysis adjusted for age, pediatric organ dysfunction score, and oxygenation index (OI) was performed to determine the independent association of MP and its derivatives 24 h after diagnosing pARDS with 28-day mortality. The association was also studied for 28 ventilator-free days (VFD-28) and the severity of pARDS in terms of OI.ResultsOut of 246 admitted with pARDS, 185 were eligible, with an overall mortality of 43.7%. Non-survivors exhibited higher severity of illness, as evidenced by higher values of MP, MPBW, and MEBW. Multivariable logistic regression analysis showed that only MEBW but not MP, MPBW, or MPCRS at 24 h was independently associated with mortality [adjusted OR: 1.072 (1.002-1.147), p = 0.044]. However, after adjusting for the type of pARDS, MEBW was not independently associated with mortality [adjusted OR: 1.061 (0.992-1.136), p = 0.085]. After adjusting for malnutrition, only MP at 24 h was found to be independently associated. Only MPCRS at 1-4 and 24 h but not MP, MPBW, or MEBW at 24 h of diagnosing pARDS was significantly correlated with VFD-28.ConclusionsNormalization of MP is better related to outcomes and severity of pARDS than non-normalized MP. Malnutrition can be a significant confounding factor in resource-limited settings.

Project description:BackgroundThe incidence of chronic lung disease is increasing, suggesting a need to explore novel ways to understand ventilator induced lung injury (VILI) in preterm infants. Mechanical power (MP) is a unifying measure of energy transferred to the respiratory system and a proposed determinant of VILI. The gold-standard method for calculating MP (geometric method) is not feasible in the clinical setting. This has prompted the derivation of simplified equations for calculating MP.ObjectiveTo validate the agreement between a simplified calculation of MP (MPSimple) and the true MP calculated using the geometric method (MPRef).MethodsMPSimple and MPRef was calculated in mechanically ventilated preterm lambs (n = 71) and the agreement between both measures was determined using intraclass correlation coefficients (ICC), linear regression, and Bland-Altman analysis.ResultsA strong linear relationship (adjusted R2 = 0.98), and excellent agreement (ICC = 0.99, 95% CI = 0.98-0.99) between MPSimple and MPRef was demonstrated. Bland-Altman analysis demonstrated a negligible positive bias (mean difference = 0.131 J/min·kg). The 95% limits of agreement were -0.06 to 0.32 J/min·kg.ConclusionsIn a controlled setting, there was excellent agreement between MPSimple and gold-standard calculations. MPSimple should be validated and explored in preterm neonates to assess the cause-effect relationship with VILI and neonatal outcomes.Impact statementMechanical power (MP) unifies the individual components of ventilator induced lung injury (VILI) and provides an estimate of total energy transferred to the respiratory system during mechanical ventilation. As gold-standard calculations of mechanical power at the bedside are not feasible, alternative simplified equations have been proposed. In this study, MP calculated using a simplified equation had excellent agreement with true MP in mechanically ventilated preterm lambs. These results lay foundations to explore the role of MP in neonatal VILI and determine its relationship with short and long term respiratory outcomes.

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Mechanical power driven SPME-SERS ultra-fast detection of illegal additives in aquaculture water.

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Mechanical power driven SPME-SERS ultra-fast detection of illegal additives in aquaculture water.

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