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PH-regulated hydrothermal synthesis and characterization of Sb4O5X2 (X = Br/Cl) and its use for the dye degradation of methyl orange both with and without light illumination.


ABSTRACT: A pH-regulated hydrothermal synthesis method was employed to synthesize Sb4O5Br2 and Sb4O5Cl2 crystallites. Characterization is done by single crystal X-ray diffraction, powder X-ray diffraction, infra-red spectroscopy, scanning electron microscopy and DFT studies. The compounds crystallize in monoclinic symmetry with a P21/c space group. Complete structural analysis of the Sb4O5Br2 compound by using single crystal X-ray diffraction data is performed for the first time and a comparative study with Sb4O5Cl2 is also discussed. The SEM study reveals that the surface morphology changes with the variation of pH for bromide compounds, wherea

SUBMITTER: Paul S 

PROVIDER: S-EPMC8984917 | biostudies-literature | 2022 Mar

REPOSITORIES: biostudies-literature