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Synthesis and Characterization of LaNi0.5Ti0.5O3 and La2NiTiO6 Double Perovskite Nanoparticles.

ABSTRACT: In the present work, LaNi0.5Ti0.5O3 and La2NiTiO6 nanoparticles were synthesized by the modified Pechini method. LaNi0.5Ti0.5O3 was calcined at 1073 K for 17 h or 100 h, while La2NiTiO6 was calcined at 1273 K for 135 h. The double perovskite calcined at 1073 K for 17 h presented orthorhombic symmetry with Pbnm space group, mean particle size was 31.9 ± 1 nm, random ordering of Ni2+ and Ti4+ cations, Néel temperature close to 15 K, and magnetic moment of 1.29 μB. By increasing the calcination time, this material showed the same symmetry and space group, a mean particle size of 50.7 ± 2 nm, short-range ordering of Ni2+ and Ti4+ cations, Néel temperature around 12 K, and magnetic moment of 0.96 μB. La2NiTiO6 presented a monoclinic crystal structure, with P21/n space group, mean particle size of 80.0 ± 5 nm, rock salt ordering of Ni2+ and Ti4+, Néel temperature of approximately 23 K, and magnetic moment of 2.75 μB.

SUBMITTER: Cordova-Calderon J 

PROVIDER: S-EPMC8999483 | biostudies-literature | 2022 Mar

REPOSITORIES: biostudies-literature

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Synthesis and Characterization of LaNi<sub>0.5</sub>Ti<sub>0.5</sub>O<sub>3</sub> and La<sub>2</sub>NiTiO<sub>6</sub> Double Perovskite Nanoparticles.

Córdova-Calderón José J   Tuza Pablo V PV   Souza Mariana M V M MMVM  

Materials (Basel, Switzerland) 20220325 7

In the present work, LaNi<sub>0.5</sub>Ti<sub>0.5</sub>O<sub>3</sub> and La<sub>2</sub>NiTiO<sub>6</sub> nanoparticles were synthesized by the modified Pechini method. LaNi<sub>0.5</sub>Ti<sub>0.5</sub>O<sub>3</sub> was calcined at 1073 K for 17 h or 100 h, while La<sub>2</sub>NiTiO<sub>6</sub> was calcined at 1273 K for 135 h. The double perovskite calcined at 1073 K for 17 h presented orthorhombic symmetry with <i>Pbnm</i> space group, mean particle size was 31.9 ± 1 nm, random ordering of Ni<  ...[more]

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