Preparation of ZnS@N-doped-carbon composites via a ZnS-amine precursor vacuum pyrolysis route.
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ABSTRACT: ZnS/carbon nanocomposites have potential electrochemical applications due to their improved conductivity and more active sites through modification of the carbon materials. Herein, we report a facile method to synthesize the nanocomposites comprising ZnS nanoparticles and nitrogen-doped carbon (ZnS@NC). The inorganic-organic hybrid ZnS-amine material ZnS(ba) (ba = n-butylamine) is synthesized on a large scale by a reflux method, which effectively shortens the reaction time while maintaining the high yield compared with the solvothermal method. Then ZnS(ba) is used as precursor for obtaining ZnS@NC nanocomposites via a vacuum pyrolysis route, in which the content of carbon and nitrogen can be controlled by adjusting the pyrolysis temperature. Further, a series of ZnS-amine hyb
SUBMITTER: Liao WH
PROVIDER: S-EPMC9042273 | biostudies-literature | 2021 Oct
REPOSITORIES: biostudies-literature
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