Waste snail shell derived heterogeneous catalyst for biodiesel production by the transesterification of soybean oil.
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ABSTRACT: A waste snail shell (Pila spp.) derived catalyst was used to produce biodiesel from soybean oil at room temperature for the first time. The snail shell was calcined at different temperatures of 400-1000 °C. The synthesized catalysts underwent XRD, SEM, TEM, EDS, FTIR, XRF, TG/DTA and N2 adsorption-desorption isotherm (BET) analysis. The major component CaO was determined at a calcination temperature of 900 °C as depicted in the XRD results. 100% conversion of soybean oil to methyl ester biodiesel was obtained, as confirmed by 1H NMR. A biodiesel yield of 98% was achieved under optimized reaction conditions such as a calcination temperature of 900 °C, a catalyst loading of 3 wt%, a reaction time of 7 h and a methanol to oil ratio of 6 : 1, and biodiesel conversi
SUBMITTER: Laskar IB
PROVIDER: S-EPMC9080767 | biostudies-literature | 2018 May
REPOSITORIES: biostudies-literature
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