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A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid.

ABSTRACT: A novel synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid which has mild conditions and low toxicity is described. This study introduces detailed synthetic protocols and characterization including GC-MS, 13C NMR and 19F NMR spectroscopy of perfluoroisobutyryl acid, perfluoroisobutyryl chloride, perfluoroisobutyl amide and perfluoroisobutyronitrile. Besides, this route is superior to the established patent and shows potential application in high voltage electrical equipment.

SUBMITTER: Wang Y 

PROVIDER: S-EPMC9088968 | biostudies-literature | 2018 Nov

REPOSITORIES: biostudies-literature

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A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid.

Wang Yi Y   Sun Mengting M   Gao Zhanyang Z   Zou Lilin L   Zhong Lingyu L   Peng Ruichao R   Yu Ping P   Luo Yunbai Y  

RSC advances 20181105 65

A novel synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid which has mild conditions and low toxicity is described. This study introduces detailed synthetic protocols and characterization including GC-MS, <sup>13</sup>C NMR and <sup>19</sup>F NMR spectroscopy of perfluoroisobutyryl acid, perfluoroisobutyryl chloride, perfluoroisobutyl amide and perfluoroisobutyronitrile. Besides, this route is superior to the established patent and shows potential application in high volt  ...[more]

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