Continuous flow synthesis of phosphate binding h-BN@magnetite hybrid material.
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ABSTRACT: Hexagonal boron nitride (h-BN) is rendered magnetically responsive in aqueous media by binding superparamagnetic magnetite nanoparticles 8.5-18.5 nm in diameter on the surface. The composite material was generated under continuous flow in water in a dynamic thin film in a vortex fluidic device (VFD) with the source of iron generated by laser ablation of a pure iron metal target in the air above the liquid using a Nd:YAG pulsed laser operating at 1064 nm and 360 mJ. Optimum operating parameters of the VFD were a rotational speed of 7.5k rpm for the 20 mm OD (17.5 mm ID) borosilicate glass tube inclined at 45 degrees, with a h-BN concentration at 0.1 mg mL-1, delivered at 1.0 mL min-1 using a magnetically stirred syringe to keep the h-BN uniformly dispersed in water pri
SUBMITTER: Mohammed Al-Antaki AH
PROVIDER: S-EPMC9091421 | biostudies-literature | 2018 Dec
REPOSITORIES: biostudies-literature
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