Molecular design and synthesis of new dithiocarbazate complexes; crystal structure, bioactivities and nano studies.

ABSTRACT: The syntheses of a new set of metal complexes MoO₂L'(CH₃OH), VOL'(CH₃O)(CH₃OH), , , SnL'Cl₂ and SnL'I₂ with a new ligand (L = (2,2'(disulfanediylbis((ethylthio)methylene)bis(hydrazin-2-yl-1-ylidene)bis(methanylylidene)) diphenol; L' = S-ethyl-3-(2-hydroxyphenyl)methylenedithiocarbazate are described along with characterization by elemental analysis, mass spectrometry, spectroscopic (IR, ¹H- and ¹³C-NMR) and TGA techniques. The crystal structures of compounds were determined by single crystal X-ray diffraction analysis and compared to powder X-ray diffraction (PXRD) patterns of the nano complexes obtained using ultrasonic methods. The PXRD results indicate that the compounds synthesized by ultraso

SUBMITTER: Yekke-Ghasemi Z 

PROVIDER: S-EPMC9091968 | biostudies-literature | 2018 Dec

REPOSITORIES: biostudies-literature