Isolation and Characterization of Cellulose Nanocrystals from Date Palm Waste.

ABSTRACT: This study presents the isolation, characterization, and kinetic analyses of cellulose nanocrystals (CNCs) from date palm waste in the United Arab Emirates. After bleaching date palm stem waste with acidified NaClO₂ and delignification via NaOH treatments, cellulose was extracted. Mineral acid hydrolysis (62 wt % H₂SO₄) was performed at 45 °C for 45 min to produce crystalline nanocellulose. Fourier transform infrared (FTIR) and chemical composition analysis confirmed the removal of noncellulosic constituents. The crystallinity index increased gradually with chemical treatments, according to the obtained X-ray diffraction (XRD) results. Thermogravimetric analysis and differential scanning calorimetry results revealed that the CNC has high thermal stability.

SUBMITTER: Raza M 

PROVIDER: S-EPMC9330260 | biostudies-literature | 2022 Jul

REPOSITORIES: biostudies-literature