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Apatitic calcium phosphate/montmorillonite nano-biocomposite: in-situ synthesis, characterization and dissolution properties.


ABSTRACT: Recently, calcium phosphate/montmorillonite composites have received attention as a synthetic bone substitutes. In this study, apatitic calcium phosphate/Montmorillonite nano-biocomposites were in-situ synthesized at 22 °C by reaction between calcium hydroxide and orthophosphoric acid in the presence of different contents of montmorillonite (MNa). Fourier Transform Infrared Spectroscopy (FTIR), X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM) and Brunauer-Emmett-Teller (BET) surface areas were used to characterize the prepared powders. The XRD results show that the composites prepared with 2 and 5 wt% MNa and sintered at 900 °C, show the formation of hydroxyapatite (HAP) structure, whereas that prepared with 10 wt% MNa leads to the formation of β-tricalcium phosphate (β-TCP)

SUBMITTER: Jamil M 

PROVIDER: S-EPMC9364031 | biostudies-literature | 2022 Aug

REPOSITORIES: biostudies-literature