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Dynamic thin film mediated slicing of boron nitride nanotubes.


ABSTRACT: A method has been developed to slice boron nitride nanotubes BNNTs under continuous flow in a vortex fluidic device (VFD), along with a method to partially purify the as received BNNT containing material. The latter involves heating the BNNTs to 600 °C followed by dispersing in a 1 : 3 isopropyl alcohol (IPA) and water mixture at 100 °C. The VFD mediated slicing of the BNNTs comprises irradiating the rapidly rotating glass tube (20 mm OD) with a pulsed Nd:YAG laser. Systematically exploring the operating parameter space of the VFD established slicing of ca. 200 μm long purified BNNTs down to 340 nm to 400 nm, in ca. 53% yield, in a 1 : 1 mixture of IPA and water, in the absence of reagents/harsh chemicals, at a flow rate of 0.45 mL min-1, a concentration of 0.1 mg

SUBMITTER: Al-Antaki AHM 

PROVIDER: S-EPMC9417105 | biostudies-literature | 2019 Dec

REPOSITORIES: biostudies-literature