Gas-solid two-phase flow (GSF) mechanochemical synthesis of dual-metal-organic frameworks and research on electrochemical properties.

ABSTRACT: As an alternative approach for conventional mechanochemical synthesis, a novel gas-solid two-phase flow (GSF) synthetic technique for the mechanochemical synthesis of dual metal-organic frameworks (DMOFs) was reported for the first time. The prepared CoMn₂(BTC)₂ was characterized by FT-IR, DTA, TG/DTG, and XRD studies. The results indicated that CoMn₂(BTC)₂ (BTC = 1,3,5-benzenetricarboxylate) was successfully synthesized after 10 min at a rate of 60 kg h^-1. CoMn₂O₄ microspheres were also prepared via the CoMn₂(BTC)₂ precursor method and characterized using FT-IR, XPS, XRD, SEM, EDS, and BET methods. The electrochemical properties of the as-prepared CoMn₂O₄ were in

SUBMITTER: Zhao J 

PROVIDER: S-EPMC9417803 | biostudies-literature | 2020 Dec

REPOSITORIES: biostudies-literature