The effectiveness of Soxhlet extraction as a simple method for GO rinsing as a precursor of high-quality graphene.
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ABSTRACT: Graphite-oxide (GO) is a valuable compound produced by the chemical oxidation of graphite. The procedure for converting graphite into GO includes two steps: oxidation and subsequent rinsing. Proper rinsing is essential to obtain processable and applicable graphite-oxide. Traditionally, the rinsing involves filtration or centrifugation; both processes are extremely time-consuming, expensive, unsafe, and produce environmentally hazardous liquid waste in large volume. This study reveals an alternative method to rinse graphite-oxide using a Soxhlet extractor. Since only the vapor of the solvent is used for washing, Soxhlet rinsing offers reuse of the same solvent for many automatic subsequent cycles, leading to considerable solvent savings, reducing pollutants and work time, and ensuring safer
SUBMITTER: Trolles-Cavalcante SYT
PROVIDER: S-EPMC9418454 | biostudies-literature | 2021 Sep
REPOSITORIES: biostudies-literature
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