Microwave-Enhanced Crystalline Properties of Zinc Ferrite Nanoparticles.

ABSTRACT: Two series of ZnFe₂O₄ mixed cubic spinel nanoparticles were prepared by a coprecipitation method, where a solution of Fe³⁺ and Zn²⁺ was alkalised by a solution of NaOH. While the first series was prepared by a careful mixing of the two solutions, the microwave radiation was used to enhance the reaction in the other series of samples. The effect of the microwave heating on the properties of the prepared particles is investigated. X-ray powder diffraction (XRD), ⁵⁷Fe Mössbauer spectroscopy and magnetometry were employed to prove the cubic structure and superparamagnetic behavior of the samples. The particle size in the range of nanometers was investigated by a transmission electron microscopy (TEM), and the N₂ adsorption measu

SUBMITTER: Ochmann M 

PROVIDER: S-EPMC9457733 | biostudies-literature | 2022 Aug

REPOSITORIES: biostudies-literature