Core-shell magnetic mesoporous N-doped silica nanoparticles: solid base catalysts for the preparation of some arylpyrimido[4,5-b]quinoline diones under green conditions.
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ABSTRACT: Nowadays, the application of solid base catalysts as a perfect replacement for homogenous basic catalysts has attracted the attention of researchers. In this study, core-shell magnetic mesoporous N-doped silica nanoparticles N(x wt%)-MSN, as a heterogeneous base catalyst, were synthesized. The N(x wt%)-MSN composite was fabricated by adding different amounts of diethanolamine as a source of nitrogen, besides using tetraethylorthosilicate as a precursor of silica. The as-prepared catalyst was employed efficiently for the synthesis of some arylpyrimido[4,5-b]quinoline-dione derivatives under green conditions. The highly efficient catalyst N(1.3 wt%)-MSN was characterized via XRD, FESEM, HRTEM, BET and XPS techniques, and the results of these analyses proved that t
SUBMITTER: Neamani S
PROVIDER: S-EPMC9476997 | biostudies-literature | 2020 Sep
REPOSITORIES: biostudies-literature
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