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Solid-Phase Synthesis of Titanium Dioxide Micro-Nanostructures.


ABSTRACT: Titanium dioxide (TiO2) micro-nanostructures are widely utilized in photochemical applications due to their unique band gaps and are of huge demand in scientific research and industrial manufacture. Herein, this work reports a controllable, facile, economical, and green solid-phase synthesis strategy to prepare TiO2 with governable morphologies containing 1D nanorods, 3D microbulks, and irregular thick plates. Specifically, Ti powders are transformed into TiO2 micro-nanostructures through dispersing them into a solid NaOH/KOH mixture with a low eutectic point, followed by grinding, heating, ion exchange, and calcination. As no solvents are utilized in the alkali treatment process, the usage of solvents is decreased and high vapor pressure is avoided. Moreov

SUBMITTER: Han XH 

PROVIDER: S-EPMC9557878 | biostudies-literature | 2022 Oct

REPOSITORIES: biostudies-literature