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Development of a modular photoreactor for the upscaling of continuous flow photochemistry† † Electronic supplementary information (ESI) available. See DOI: https://doi.org/10.1039/d2re00310d

ABSTRACT: The upscaling of biphasic photochemical reactions is challenging because of the inherent constraints of liquid–gas mixing and light penetration. Using semi-permeable coaxial flow chemistry within a modular photoreactor, the photooxidation of the platform chemical furfural was scaled up to produce routinely 29 gram per day of biobased building block hydroxybutenolide, a precursor to acrylate alternatives. An easily-built, user-friendly modular photoreactor enables optimization and upscaling of flow photooxidation.

SUBMITTER: Hermens J

PROVIDER: S-EPMC9594834 | biostudies-literature | 2022 Sep

REPOSITORIES: biostudies-literature

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